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Wednesday, August 4, 2004 - 9:10 AM
SES 14.2

Optimization of Thermally Sprayed Metallic Nanocomposite Coatings

J. Colmenares, Central University of Venezuela, Caracas, Venezuela; M. Rodriguez, Universidad Central de Venezuela, Caracas, Venezuela; A. Scagni, Plasmatec Ingenieros, C.A., Caracas, Venezuela

The aim of this work was to find the optimal parameters for spraying Super Hard Steel (SHS) 717 Iron based powder. SHS 717 is a glass forming alloy produced by atomization techniques. When sprayed, a mixed structure is achieved consisting of amorphous metallic glass with regions containing nanocrystalline grains. We use a factorial experimental design 32 to obtain the optimum parameters. The operational parameters under study were Oxygen/Fuel ratio and powder spray rate for High Velocity Oxy-Fuel (HVOF) process using a JP-5000 gun. The different combinations of parameters were tested for abrasion and sliding wear tests performed according to ASTM G-65 and G-99-95ª respectively. The microstructure and composition of the coatings, failure and worn surface were evaluated using Optical (OM) and Scanning Electron Microscopy (SEM) as well as X-Ray energy Dispersive Spectroscopy (EDX). The optimal parameters were found using a regression analysis and a multi analysis of variance (manova).

Summary: The aim of this work was to find the optimal parameters for spraying Super Hard Steel (SHS) 717 Iron based nanocomposite alloy using two different thermal spray processes. The operational parameters were tested for abrasion and microhardness. The optimal parameters were found using a regression analysis and analysis of variance.