Metavolcanic Carbonate-Active Binder (MCAB): A Catalytically Tunable, Carbon-Negative Concrete System

Mr. Edwin Maina , Portland State University, Portland, OR
Abstract
This paper introduces the Metavolcanic Carbonate-Active Binder (MCAB), a concrete system formulated from finely milled metavolcanic-pozzolan co-blended with magnesium-silicate seeds (e.g., forsterite/serpentine) and sub-percent carbonate-catalyst ensembles (calcium/magnesium nano-carbonates with trace iron). The working hypothesis is that mesoscale nucleation control and interfacial ion transport can be tuned to accelerate the co-precipitation of carbonate minerals specifically calcite, aragonite, and hydromagnesite during curing, yielding predictable CO2 uptake while maintaining robust structural performance.
To explore this, a kinetic model is developed that links: (i) catalyst loading (0.1-1.0 wt%), (ii) ash reactivity index, and (iii) time-temperature-humidity profiles to the carbonation mineralization rate and early-age compressive strength. The model generates design maps targeting 10-20% CO2 uptake by mass within 24 hours, with predicted strength retention exceeding 80% of standard concrete despite a 70-90% replacement of Portland clinker.
The validation plan involves:

  1. Synthesizing MCAB pastes at 0.30–0.45 water/binder ratios with 70–90% clinker substitution.
  2. Implementing both controlled CO2 curing (0.1–1 bar partial pressure) and ambient carbonation protocols.
  3. Quantifying CO2 uptake via thermogravimetric analysis (TGA/DSC) and a closed-loop CO2 mass balance system.
  4. Resolving carbonate polymorphs and silicate hydrate reaction products using X-ray diffraction with ATR-FTIR.
  5. Assessing evolution of the pore structure via Mercury Intrusion Porosimetry and N2 sorption.
  6. Measuring mechanical properties (compressive strength, fracture energy) and key durability indicators (chloride diffusion, sulfate resistance).

Anticipated outcomes from this research include: (a) tunable, catalyst-dependent mineralization kinetics; (b) 80% retention of the control compressive strength at 24 hours, despite high clinker replacement levels; and (c) an optimized process window (catalyst concentration, CO2 partial pressure, curing temperature) that maximizes carbon uptake without inducing micro-cracking or compromising long-term integrity. MCAB targets a ”drop-in” decarbonization solution for precast and cast-in-place workflows, translating laboratory design maps into production-ready curing recipes that deliver measurable, verifiable CO2 removal alongside structural reliability for the global construction industry.