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Tuesday, May 15, 2007 - 2:30 PM

Microstructure Characterization and Property of Plasma Sprayed Nanostructured TBCs

Q. Li, S. Li, W. Yang, Beijing Aeronautical Manufacturing Technology Research Institute, Beijing, China; J. Wu, Wuhan Research Institute of Materials Protection, Wuhan, China

The technology and thermal shock properties and thermal conductivity of plasma sprayed nanostructured yttria-stabilized zirconia thermal barrier coatings are studied in this paper. The TBCs  on  the  substrate of  Ni3Al  based  alloy  IC-10 were fabricated by using of the nanostructured  yttria-stabilized  zirconia  powder under certain plasma  spraying  conditions. By manipulating plasma spray process, the nanostructured TBCs were obtained.  The  specimens  were  thermally  shocked  from   1000C,  1100 C  and  1200C  to  the water which temperature was about 20C  and  the morphology  and  microstructure of  the  TBCs were  evaluated  by  light  microscopy,  scanning  electron  microscopy (SEM)  and  transmission  electron  microscopy(TEM).  The thermal diffusivity was tested by a laser pulse method. The  results showed that the nanostructured TBCs  had  a  more  than  30%  reduction  in  thermal  conductivity  and the  thermo shock  lifetimes  were  much  longer  than  that  of  the  conventional  TBCs.

Summary: The technology and thermal shock properties and thermal conductivity of plasma sprayed nanostructured yttria-stabilized zirconia thermal barrier coatings are studied in this paper. The TBCs on the substrate of Ni3Al based alloy IC-10 were fabricated by using of the nanostructured yttria-stabilized zirconia powder under certain plasma spraying conditions. By manipulating plasma spray process, the nanostructured TBCs were obtained. The specimens were thermally shocked from 1000, 1100 and 1200 to the water which temperature was about 20 and the morphology and microstructure of the TBCs were evaluated by light microscopy, scanning electron microscopy (SEM) and transmission electron microscopy(TEM). The thermal diffusivity was tested by a laser pulse method. The results showed that the nanostructured TBCs had a more than 30% reduction in thermal conductivity and the thermo shock lifetimes were much longer than that of the conventional TBCs.