High temperature hot corrosion behavior of selected thermally sprayed coatings in an aggressive environment at 690 °C

Monday, May 27, 2019
Dr. Zdeněk Česánek , Research and testing Institute in Pilsen Ltd., Pilsen, Czech Republic
Dr. Radek Musalek , Institute of Plasma Physics AS CR, Prague, Czech Republic
Dr. Frantisek Lukac , Institute of Plasma Physics, Czech Academy of Sciences, Prague, Czech Republic
Dr. Šárka Houdkova , Research and testing Institute in Pilsen Ltd., Pilsen, Czech Republic
Mrs. Kateřina Kopelentová , Research and testing Institute in Pilsen Ltd., Pilsen, Czech Republic
Mr. Jan Schubert , Research and testing Institute in Pilsen Ltd., Pilsen, Czech Republic
This study is focused on hot corrosion evaluation of selected thermal sprayed coatings. Cr3C2-25%NiCr, Stellite 6, NiCrBSi and Hastelloy C-276 was sprayed to the substrate material 1.4923. This material is used as an efficient construction material for components of power equipment. All tested coatings were sprayed using HP / HVOF (High Pressure / High Velocity Oxygen Fuel) technology.

Hot corrosion studies were performed in a molten salt environment typical for coal-fired boilers. All coatings was exposited Na2SO4 82 % Fe2 (SO4)3 environment at 690 °C under cyclic condition. Each cycle consisted 1h heating in silicon carbide tube furnace followed by 20 min of cooling. The weight change measurement was performed after each cycle to establish the corrosion kinetics. Scanning electron microscopy (SEM), elemental analysis (EDS) and optical microscopy (OM) technique were used to analyse the corrosion mechanism.

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