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Monday, September 24, 2007

Characterization of Nitinol Material Behavior for the Design and Validation of Medical Implants

K. E. Perry, P. Labossiere, ECHOBIO, LLC., Bainbridge Island, WA

Phase shifted moiré interferometry is used to measure full-field strain under precise loading conditions for superelastic and shape memory nitinol component test samples.  Uniaxial tension and four point bend loading is accomplished with a single sample geometry fabricated with commercially available tubing, similar to what is used for medical implants.  Material property changes as a function of cyclic loading for a range of loading intensities are presented for two process methods.  Our results are used to demonstrate typical thermomechanical processing effects including the presence of R-phase and thermally recoverable strain on the evolution of performance properties of medical components.  Compact tension samples with sharp fatigue pre-cracks will also be discussed to provide further insight into the initiation and growth of critical flaws from process and design related stress concentration conditions.  Experimental data from the full-field, in situ interferometric measurement technique provides a self-consistent method for calibrating finite element analysis results and validating implantable medical device components.

Summary: Phase shifted moiré interferometry is used to measure full-field strain under precise loading conditions for superelastic and shape memory nitinol component test samples. Uniaxial tension and four point bend loading is accomplished with a single sample geometry fabricated with commercially available tubing, similar to what is used for medical implants. Material property changes as a function of cyclic loading for a range of loading intensities are presented for two process methods. Our results are used to demonstrate typical thermomechanical processing effects including the presence of R-phase and thermally recoverable strain on the evolution of performance properties of medical components. Compact tension samples with sharp fatigue pre-cracks will also be discussed to provide further insight into the initiation and growth of critical flaws from process and design related stress concentration conditions. Experimental data from the full-field, in situ interferometric measurement technique provides a self-consistent method for calibrating finite element analysis results and validating implantable medical device components.